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Título: | A novel, simple and rapid route to the synthesis of boron cabonitride nanosheets: Combustive gaseous unfolding |
Autor: | Jalaly, M.; Gotor, F.J. CSIC ORCID ; Sayagués, María Jesús CSIC ORCID | Fecha de publicación: | 2017 | Editor: | Nature Publishing Group | Citación: | Scientific Reports 7: 3453 (2017) | Resumen: | The ternary compound boron carbonitride (BCN) was synthesized in the form of few-layer nanosheets through a mechanically induced self-sustaining reaction (MSR). Magnesium was used to reduce boron trioxide in the presence of melamine in a combustive manner. The process to form the nanostructured material was very rapid (less than 40¿min). The prepared powder was investigated by various techniques such as X-ray diffraction (XRD), Fourier Transform infrared (FTIR), Micro-Raman spectroscopy, X-ray photoelectron spectroscopy (XPS), high-resolution transmission electron microscopy (HRTEM), and electron energy loss spectroscopy (EELS). The thermal stability and the optical behavior of the BCN nanosheets were also studied by thermal analysis and UV-vis spectroscopy, respectively. The formation mechanism of the nanosheet morphology was described in detail. | URI: | http://hdl.handle.net/10261/159060 | DOI: | 10.1038/s41598-017-03794-7 | Identificadores: | doi: 10.1038/s41598-017-03794-7 issn: 2045-2322 |
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