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Título: | Sonochemical synthesis of a novel nanoscale 1D lead(II) [Pb2(L)2(I)4]n coordination Polymer, survey of temperature, reaction time parameters |
Autor: | Hayati, Payam CSIC ORCID; Suárez-García, Salvio CSIC ORCID; Gutiérrez, Angel; Ruiz Molina, Daniel CSIC ORCID; Morsali, Ali; Reza Rezvani, Ali | Fecha de publicación: | 2018 | Editor: | Elsevier | Citación: | Ultrasonics Sonochemistry 42: 320-326 (2018) | Resumen: | One new lead(II) coordination supramolecular complex (CSC) (1D), [Pb2(L)2(I)4]n, L = C4H6N2 (1-methyl imidazole), has been synthesized under different experimental conditions. Micrometric crystals (bulk) or nano-sized materials have been obtained depending on using the branch tube method or sonochemical irradiation. All materials have been characterized by scanning electron microscopy (SEM), powder X-ray diffraction (PXRD) and FT-IR spectroscopy. Single crystal X-ray analyses on complex 1 showed that Pb2+ ion is 4-coordinated. Topological analysis shows that the complex 1 is 2,3,5C2 net. Finally, the role of reaction time and temperature on the growth and final morphology of the structures obtained by sonochemical irradiation have been studied. | Versión del editor: | https://doi.org/10.1016/j.ultsonch.2017.11.033 | URI: | http://hdl.handle.net/10261/199832 | DOI: | 10.1016/j.ultsonch.2017.11.033 | ISSN: | 1350-4177 | E-ISSN: | 1873-2828 |
Aparece en las colecciones: | (CIN2) Artículos |
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