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Título: | Electric current activated sintering (ECAS) of undoped and titanium-doped BiFeO3 bulk ceramics with homogeneous microstructure |
Autor: | Bernardo, M. S. CSIC ORCID; Jardiel, Teresa CSIC ORCID ; Caballero Cuesta, Amador CSIC ORCID; Bram, M.; González Julián, Jesús CSIC ORCID; Peiteado, Marco CSIC ORCID | Palabras clave: | ECAS sintering Flash and FAST sintering BiFeO3 Homogeneous microstructure DC electricfield AC electricfield |
Fecha de publicación: | 2019 | Editor: | Elsevier | Citación: | Journal of the European Ceramic Society 39: 2042- 2049 (2019) | Resumen: | [EN] BiFeO ceramics have been consolidated applying an electric current activated/assisted sintering (ECAS) methodology under different electrical conditions. DC experiments produce a flash sintering regime by which the bulk cylindrical specimens densify in a few seconds; however, this goes together with a strong localization of the current flow within the material, leading to a dramatic lack of microstructural and compositional homogeneity. The situation changes under the alternate field; a more gradual FAST (Field Assisted Sintering) event is produced which allows the attainment of an exceptional microstructural homogeneity through the whole sintered compacts. Upon Ti-doping the overall diffusivity of the system is delayed but the AC conditions again yield a remarkable microstructural homogeneity in the consolidated material, this time even at the nanoscale level. Accordingly, bulk BiFeO ceramics with homogeneous micro-nanostructure can be successfully prepared by an ECAS methodology and at lower temperatures and much shorter times than by conventional solid-state sintering. | Versión del editor: | http://dx.doi.org/10.1016/j.jeurceramsoc.2019.01.045 | URI: | http://hdl.handle.net/10261/211774 | DOI: | 10.1016/j.jeurceramsoc.2019.01.045 | Identificadores: | doi: 10.1016/j.jeurceramsoc.2019.01.045 e-issn: 1873-619X issn: 0955-2219 |
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