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Título: | Derivatization of carbohydrates for GC and GC–MS analyses |
Autor: | Ruiz-Matute, Ana I. CSIC ORCID ; Hernández-Hernández, Oswaldo CSIC ORCID ; Rodríguez-Sánchez, Sonia CSIC; Sanz, M. Luz CSIC ORCID ; Martínez-Castro, Isabel CSIC | Palabras clave: | Derivatization Carbohydrates GC GC-MS |
Fecha de publicación: | may-2011 | Editor: | Elsevier | Citación: | Journal of Chromatography B 879(17-18): 1226-1240 (2011) | Resumen: | GC and GC–MS are excellent techniques for the analysis of carbohydrates; nevertheless the preparation of adequate derivatives is necessary. The different functional groups that can be found and the diversity of samples require specific methods. This review aims to collect the most important methodologies currently used, either published as new procedures or as new applications, for the analysis of carbohydrates. A high diversity of compounds with diverse functionalities has been selected: neutral carbohydrates (saccharides and polyalcohols), sugar acids, amino and iminosugars, polysaccharides, glycosides, glycoconjugates, anhydrosugars, difructose anhydrides and products resulting of Maillard reaction (osuloses, Amadori compounds). Chiral analysis has also been considered, describing the use of diastereomers and derivatives to be eluted on chiral stationary phases. | Descripción: | 15 páginas, 5 figuras, 3 tablas. | Versión del editor: | http://dx.doi.org/10.1016/j.jchromb.2010.11.013 | URI: | http://hdl.handle.net/10261/49791 | DOI: | 10.1016/j.jchromb.2010.11.013 | ISSN: | 1570-0232 |
Aparece en las colecciones: | (CIAL) Artículos (IQOG) Artículos |
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