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Journal Article

Continuous synthesis of nanostructured silica based materials in a gas–liquid segmented flow tubular reactor

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Mezzavilla,  Stefano
Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Schüth,  Ferdi
Research Department Schüth, Max-Planck-Institut für Kohlenforschung, Max Planck Society;

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Citation

Knossalla, J., Mezzavilla, S., & Schüth, F. (2016). Continuous synthesis of nanostructured silica based materials in a gas–liquid segmented flow tubular reactor. New Journal of Chemistry, 40(5), 4361-4366. doi:10.1039/C5NJ03033A.


Cite as: https://hdl.handle.net/11858/00-001M-0000-002B-4A98-2
Abstract
A continuous synthesis of several spherical silica structures – by means of a gas–liquid segmented flow tubular reactor – is reported. Specifically, as proof of concept, we showed that 300–400 nm mesoporous core–shell spheres (SiO2@mSiO2), mesoporous spheres (mSiO2) as well gold-encapsulated spheres (Au@SiO2) can be effectively produced in a continuous manner in a tubular reactor. Thus, the successful conversion of classical batch methods to continuous processes opens new possibilities for the up-scaled synthesis of advanced nanostructured materials.