A statistical Plackett-Burman design of the thermal process in the synthesis of the Bi-2223 HTSC
- Author
- Isabel Van Driessche (UGent) , F Persyn, Lucien Fiermans and Serge Hoste (UGent)
- Organization
- Abstract
- In this study, the most significant parameters in the thermal process for the preparation of high-quality Bi-2223 HTSCs are determined using a statistical Plackett-Burman screening design. This enabled us to obtain a quick and objective evaluation, where the significant parameters could be unambiguously defined, accounting for interactions with other parameters. Using the optimal conditions of the thermal process and starting from a spray dried nitrate solution with nominal composition Bi:Pb:Sr:Ca:Cu = 1.5:0.5:2:3:4, a more than 96% pure Bi-2223 phase (relative to the Bi-2212 phase) could be synthesized in a minimal thermal process of 5 h calcination at 650 degrees C and 60 h sintering at 855 degrees C.
- Keywords
- HIGH-TC PHASE, CU-O SYSTEM, BI
Citation
Please use this url to cite or link to this publication: http://hdl.handle.net/1854/LU-190379
- MLA
- Van Driessche, Isabel, et al. “A Statistical Plackett-Burman Design of the Thermal Process in the Synthesis of the Bi-2223 HTSC.” SUPERCONDUCTOR SCIENCE & TECHNOLOGY, vol. 9, no. 10, 1996, pp. 843–48.
- APA
- Van Driessche, I., Persyn, F., Fiermans, L., & Hoste, S. (1996). A statistical Plackett-Burman design of the thermal process in the synthesis of the Bi-2223 HTSC. SUPERCONDUCTOR SCIENCE & TECHNOLOGY, 9(10), 843–848.
- Chicago author-date
- Van Driessche, Isabel, F Persyn, Lucien Fiermans, and Serge Hoste. 1996. “A Statistical Plackett-Burman Design of the Thermal Process in the Synthesis of the Bi-2223 HTSC.” SUPERCONDUCTOR SCIENCE & TECHNOLOGY 9 (10): 843–48.
- Chicago author-date (all authors)
- Van Driessche, Isabel, F Persyn, Lucien Fiermans, and Serge Hoste. 1996. “A Statistical Plackett-Burman Design of the Thermal Process in the Synthesis of the Bi-2223 HTSC.” SUPERCONDUCTOR SCIENCE & TECHNOLOGY 9 (10): 843–848.
- Vancouver
- 1.Van Driessche I, Persyn F, Fiermans L, Hoste S. A statistical Plackett-Burman design of the thermal process in the synthesis of the Bi-2223 HTSC. SUPERCONDUCTOR SCIENCE & TECHNOLOGY. 1996;9(10):843–8.
- IEEE
- [1]I. Van Driessche, F. Persyn, L. Fiermans, and S. Hoste, “A statistical Plackett-Burman design of the thermal process in the synthesis of the Bi-2223 HTSC,” SUPERCONDUCTOR SCIENCE & TECHNOLOGY, vol. 9, no. 10, pp. 843–848, 1996.
@article{190379,
abstract = {{In this study, the most significant parameters in the thermal process for the preparation of high-quality Bi-2223 HTSCs are determined using a statistical Plackett-Burman screening design. This enabled us to obtain a quick and objective evaluation, where the significant parameters could be unambiguously defined, accounting for interactions with other parameters. Using the optimal conditions of the thermal process and starting from a spray dried nitrate solution with nominal composition Bi:Pb:Sr:Ca:Cu = 1.5:0.5:2:3:4, a more than 96% pure Bi-2223 phase (relative to the Bi-2212 phase) could be synthesized in a minimal thermal process of 5 h calcination at 650 degrees C and 60 h sintering at 855 degrees C.}},
author = {{Van Driessche, Isabel and Persyn, F and Fiermans, Lucien and Hoste, Serge}},
issn = {{0953-2048}},
journal = {{SUPERCONDUCTOR SCIENCE & TECHNOLOGY}},
keywords = {{HIGH-TC PHASE,CU-O SYSTEM,BI}},
language = {{eng}},
number = {{10}},
pages = {{843--848}},
title = {{A statistical Plackett-Burman design of the thermal process in the synthesis of the Bi-2223 HTSC}},
volume = {{9}},
year = {{1996}},
}