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タイトル: | Formation of Bi,Pb-2223 and microstructural evolution in Pb-Ca-Cu deposited Bi-2212(001) single crystal by heat treatment |
著者: | Kajihara, T. Shimada, Y. Hata, S. Ikeda, K. Nakashima, H. Matsumoto, A. Mochiku, T. Kitaguchi, H. Doi, T. |
著者名の別形: | 土井, 俊哉 |
キーワード: | Bi, Pb-2223 Bi-2212 single crystal Pb-Ca-Cu film Phase transformation Heat treatment Scanning electron microscopy Scanning transmission electron maicroscopy |
発行日: | 2013 |
出版者: | Elsevier B.V. |
誌名: | Physics Procedia |
巻: | 45 |
開始ページ: | 69 |
終了ページ: | 72 |
抄録: | In order to study the mechanism of phase transformation from Bi-2212 to Bi-2223, we fabricated Pb-Ca-Cu deposited Bi-2212 (001) single crystals as precursors of the Bi, Pb-2223 phase. These single crystals were heated in a sintered Bi-Pb-Sr-Ca-Cu-O pellet, and microstructure was observed by analytical electron microscopy. As a result of the microstructural observation around the Bi, Pb-2223 phase, two formation paths of Bi, Pb-2223 were recognized. One is the formation from a liquid phase which is formed by Bi-2212 and melting of the secondary phases such as (Ca, Sr)2PbO4 and CuO. The other is the growth of Bi, Pb-2223 into Bi-2212 phase by diffusion of Pb, Ca and Cu atoms along the 〈hk0〉 directions of Bi-2212. |
記述: | 25th International Symposium on Superconductivity, ISS 2012 ; 3 December 2012 through 5 December 2012 ; Tokyo |
著作権等: | © 2013 The Authors. Published by Elsevier B.V. Open access under CC BY-NC-ND license. |
URI: | http://hdl.handle.net/2433/235666 |
DOI(出版社版): | 10.1016/j.phpro.2013.04.054 |
出現コレクション: | 学術雑誌掲載論文等 |
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