Geochemical and isotopic constraints on the diagenetic history of a massive stratal, late Cambrian (Royer) dolomite, Lower Arbuckle Group, Slick Hills, SW Oklahoma, USA
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Re-evaluation and optimisation of dissolution methods for strontium isotope stratigraphy based on chemical leaching of carbonate certificated reference materials
2020, Microchemical JournalCitation Excerpt :The dolostone reacts very slowly when dissolved in 1% HAc, therefore stronger acid strength (2.5% HAc) is employed. To verify the effectiveness of ammonium acetate preleaching in removing Sr contamination from clay minerals [16, 34], the samples were firstly leached in 10 mL ammonium acetate in step 1. Sr dissolved in sequential dilute weak acid
Coupled δ<sup>44/40</sup>Ca, δ<sup>88/86</sup>Sr, and <sup>87</sup>Sr/<sup>86</sup>Sr geochemistry across the end-Permian mass extinction event
2019, Geochimica et Cosmochimica ActaCitation Excerpt :We employed HAc solutions with concentrations of 0.25%, 1%, and 5%. Subsamples of micro-drilled powders (∼200 mg/sample) were weighed into acid-cleaned 50 mL centrifuge tubes and first reacted with ∼25 mL of 1 N ammonium acetate (NH4Ac, buffered to pH = 8.2) to isolate surface-adsorbed phases and other exchangeable cations (Gao, 1990; Bailey et al., 2000). The remaining residues were then sequentially reacted with ∼15 mL of 0.25%, 1%, and 5% HAc.
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Previous address: Department of Geology, Central-South University of Technology, Changsha, Hunan 410012, The People's Republic of China.