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Characterization of Nb interface segregation during welding thermal cycle in microalloyed steel by atom probe tomography
journal contribution
posted on 2018-12-01, 00:00 authored by H H Wang, Jiangting Wang, Z Tong, Peter HodgsonPeter Hodgson, X L Wan, K M Wu, R Wei, Ilana TimokhinaCoarse-grained, welding heat-affected zone microstructure was simulated in a Nb-bearing microalloyed steel. The granular bainite with a great number of martensite-austenite (M-A) constituents was the predominant phase. Using atom probe tomography (APT), the distributions of niobium at prior austenite grain boundary (PAGB), ferrite/martensite-austenite (M-A) constituent interface (FMAI), and ferrite/ferrite interface (FFI) were investigated. The binding energy of Nb atom and vacancy was predicted to be 0.45 eV, indicating that Nb segregation by welding thermal cycle is probably a result of the nonequilibrium mechanism. The maximum enrichment of Nb was found at FMAI with enrichment factor of 3.50. Intermediate enrichment of Nb was at PAGB with enrichment factor of 3.12. The interfacial excess of Nb solute element ГNbat PAGB determined by APT was 0.27 × 1019atoms/m2. The segregation energy was calculated to be 22.91 kJ/mol. The minimum enrichment of Nb was at FFI with an enrichment factor of 1.80.
History
Journal
Metallurgical and materials transactions AVolume
49Issue
12Pagination
6224 - 6230Publisher
SpringerLocation
Cham, SwitzerlandPublisher DOI
ISSN
1073-5623Language
engPublication classification
C1 Refereed article in a scholarly journalCopyright notice
2018, The Minerals, Metals & Materials Society and ASM InternationalUsage metrics
Keywords
Nb Interface SegregationWelding Thermal CycleMicroalloyed Steelmartensite-austenite (M-A)atom probe tomography (APT)prior austenite grain boundary (PAGB)ferrite\/martensite-austenite (M-A)(FMAI)ferrite\/ferrite interface (FFI)Science & TechnologyTechnologyMaterials Science, MultidisciplinaryMetallurgy & Metallurgical EngineeringMaterials ScienceHEAT-AFFECTED ZONEAUSTENITIC STAINLESS-STEELGRAIN-BOUNDARY SEGREGATIONNIOBIUMMICROSTRUCTURETRANSFORMATIONTOUGHNESSSOLUTEVANADIUMGROWTHMechanical Engineering
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