Qualitative and quantitative characterization of a coal power plant waste by TG/DSC/MS, XRF and XRD
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Fernández Ferreras, Josefa; González Martínez, Fernando; Pesquera González, Carmen; Neves Junior, Alex; Mendes Viana, Marcelo; Dweck, JoFecha
2016-08Derechos
© Springer-Akadémiai Kiadó.The final publication is available at Springer via http://dx.doi.org/10.1007/s10973-016-5270-8
Publicado en
Journal of Thermal Analysis and Calorimetry, 2016, 125(2), 703–710
Editorial
Springer
Palabras clave
Coal power plant
Dry desulphurization
Hydrated lime
TG/MS
XRD
XRF
Resumen/Abstract
SO2 removal from coal-fired power plant flue gases can be done by dry, semi-dry or wet desulphurization processes, using limestone or lime-containing products as sorbents. In a Brazilian coal power plant, there is a dry desulphurization unit to capture SO2 with hydrated lime from the combustion gases. A part of the flying ashes produced is mixed with the bottom coal ashes and the spent sulphated product generated after SO2 capture. This residual solid blend is then buried in a non-productive area, from which coal was already extracted and is studied in this work. According to the authors’ experience in the development and characterization of adsorbents for low temperature dry desulphurization processes and in thermogravimetric analysis, this paper shows and discusses a method which was developed to characterize qualitatively and quantitatively the chemical and mineral composition of this waste by using thermogravimetry coupled with mass spectrometry, X-ray fluorescence and X-ray diffraction, to preview new potential industrial applications for this waste.
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