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Nanoprecipitates in single-crystal molybdenum-alloy nanopillars detected by TEM and atom probe tomography

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Gerstl,  Stephan S. A.
Electron Microscopy of Eidgenössische Technische Hochschule Zurich (EMEZ), 8093 Zurich, Switzerland;
Microstructure Physics and Alloy Design, Max-Planck-Institut für Eisenforschung GmbH, Max Planck Society;

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Citation

Oveisi, E., Bártová, B., Gerstl, S. S. A., Zimmermann, J., Marichal, C., Van Swygenhoven, H., et al. (2013). Nanoprecipitates in single-crystal molybdenum-alloy nanopillars detected by TEM and atom probe tomography. Scripta Materialia, 69(1), 41-44. doi:10.1016/j.scriptamat.2013.03.013.


Cite as: https://hdl.handle.net/21.11116/0000-0001-E2A0-A
Abstract
Transmission electron microscopy (TEM) supported by various chemical analyses techniques as well as atom probe tomography is applied to characterize newly identified nanosized precipitates in Mo-alloy nanopillars that were prepared by directional solidification. It is shown that the α-Mo matrix contains Al-enriched face-centred cubic precipitates which have a 4.12 Å lattice parameter, and exhibit a Kurdjumov-Sachs crystallographic orientation relationship with the matrix. Such precipitates could be responsible for the unusual behaviour of the pillars during compression tests.© 2013 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.